This BB cream formulation was designed to provide superior broad spectrum (SPF/PFA <3), label SPF 40 performance. SolaStay® S1 provides very rapid and efficient excited state quenching of Avobenzone and also mitigates the photocatalytic and reactive oxygen species generating activities of the oxides to improve sunscreen performance. HallBrite® BHB, Sensolene® and HallTress® DIBA Special contribute to UV filter solubility and enhance product feel. Eurol® BT contributes its antiaging, skin elasticizing, anti-oxidant and moisturizing properties. This formulation was subjected to in vitro analysis and delivered SPF ~45 , PFA (PPD) ~21 performance with critical wavelength 382 nm.
Phase | INCI Name [INN/USAN] (Other Information) | Trade Name | % Wt | Function |
---|---|---|---|---|
A | Ethylhexyl Methoxycrylene | SolaStay® S1* | 2.00 | Photostabilizer |
Ethylhexyl Olivate | SENSOLENE® | 2.00 | Multifunctional Lipid | |
Diisobutyl Adipate | HALLTRESS® DIBA SPECIAL | 5.00 | Sunscreen Solvent / Emollient | |
Butyloctyl Salicylate | HALLBRITE® BHB* | 5.00 | Sunscreen Solvent / Emollient | |
Ethylhexyl Salicylate [Octisalate] | 5.00 | UV Filter / Sunscreen Agent | ||
B | Iron Oxides (yellow) (CI 77492), Triethoxycaprylylsilane | 1.30 | Pigment | |
Iron Oxides (red) (CI 77491), Triethoxycaprylylsilane | 0.42 | Pigment | ||
Iron Oxides (black) (CI 77499), Triethoxycaprylylsilane | 0.13 | Pigment | ||
C | Titanium Dioxide [Titanium Dioxide] (CI 77891), Triethoxycaprylylsilane | 5.00 | UV Filter / Sunscreen Agent | |
Ethylhexyl Triazone | 1.15 | UV Filter / Sunscreen Agent | ||
D | VP/Eicosene Copolymer | 1.00 | Film Former | |
Glyceryl Stearate | HALLSTAR® GMS PURE | 1.45 | Emulsifier | |
PEG-100 Stearate | HALLSTAR® PEG 4400 MS | 1.50 | Emulsifier | |
Potassium Cetyl Phosphate, Hydrogenated Palm Glycerides | 2.00 | Emulsifier | ||
E | Butyl Methoxydibenzoylmethane [Avobenzone] | 2.50 | UV Filter / Sunscreen Agent | |
F | Water (Aqua) (deionized) | up to 100 | Volatile Carrier | |
Glycerin | 3.00 | Humectant | ||
Disodium EDTA | 0.05 | Chelating Agent | ||
Xanthan Gum (pharma grade) | 0.25 | Thickener (Aqueous) | ||
G | Preservative | a.n. | Preservative | |
Olea Europaea (Olive) Leaf Extract, Water | EUROL® BT | 0.50 | Multifunctional Active Ingredient | |
Acrylamide/Sodium Acryloyldimethyltaurate Copolymer, Isohexadecane, Polysorbate 80 | 1.80 | Viscosity Increasing Agent (Aqueous) | ||
Cyclopentasiloxane | 2.00 | Feel Modification / Enhancement | ||
Aluminum Starch Octenylsuccinate | 2.00 | Deoiling Agent |
1 | In secondary vessel combine phase A, start mixing, add phase B to phase A and, when uniform, add phase C to phase AB. |
2 | Heat this oil phase ABC to 80°C and then add phase D to it.. |
3 | When phase ABCD is homogeneous, add phase E to it and mix until phase E is fully dissolved. |
4 | To the main vessel add Water and Glycerin of phase F, start mixing, add the Disodium EDTA and then add Xanthan Gum. |
5 | Heat phase F to 75°C with continued mixing and ensure it is homogeneous. |
6 | When both phases are at designated temperatures, slowly add phase ABCDE to phase F with prop mixing and then homogenize for 3 minutes. |
7 | Start cooling batch with center stir (prop) mixing and when < 50°C, add phase G items one by one to it with continued mixing. |
8 | Replace any water lost to evaporation and mix batch until smooth. |
Appearance | Light brown thick lotion (cream) |
Viscosity (Brk, RVDV-II, T-D, 20 rpm, after 24 h at room temperature; mPa·s) | 11000 - 18500 |
pH | 5.5 - 6.0 |
*Patented and Patent Pending
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