This sunscreen lotion is Avobenzone-, Oxybenzone- and Octocrylene-free and uses SolaStay® S1 to mitigate the photocatalytic and reactive oxygen species generating activities of the oxide. It was subjected to in vitro analysis and delivered SPF ~ 60, PFA (PPD) ~ 8 performance with critical wavelength 375 nm.
Phase | INCI Name [INN/USAN] (Other Information) | Trade Name | % Wt | Function |
---|---|---|---|---|
A | Caprylic/Capric Triglyceride | 3.00 | Sunscreen Solvent | |
Ethylhexyl Methoxycinnamate [Octinoxate] | 7.50 | UV Filter / Sunscreen Agent | ||
Ethylhexyl Methoxycrylene | SolaStay® S1* | 3.00 | Photostabilizer | |
Ethylhexyl Olivate | SENSOLENE® | 5.00 | Multifunctional Lipid | |
B | 4-Methylbenzylidene Camphor [Enzacamene] | 4.00 | UV Filter / Sunscreen Agent | |
Titanium Dioxide [Titanium Dioxide], Aluminum Hydroxide (60 nm primary particle size) | 4.10 | UV Filter / Sunscreen Agent | ||
C | VP/Eicosene Copolymer | 1.00 | Film Former | |
Glyceryl Stearate | HALLSTAR® GMS PURE | 1.50 | Emulsifier | |
PEG-100 Stearate | HALLSTAR® PEG 4400 MS | 1.60 | Co-emulsifier | |
Potassium Cetyl Phosphate, Hydrogenated Palm Glycerides | 1.65 | Emulsifier | ||
D | Water (Aqua) (deionized) | up to 100 | Volatile Carrier | |
Disodium EDTA | 0.05 | Chelating Agent | ||
Acrylates/C10-30 Alkyl Acrylate Crosspolymer | 0.24 | Thickener (Aqueous) | ||
E | Potassium Hydroxide | 1.21 | pH Adjuster | |
F | Glycerin | 3.00 | Humectant | |
Preservative | a.n. | Preservative | ||
G | Cyclopentasiloxane | 5.00 | Feel Modification / Enhancement | |
Aluminum Starch Octenylsuccinate | 2.00 | Feel Modification / Enhancement |
1 | To a secondary vessel add phase A, start mixing and slowly add phase B components individually to phase A with continued mixing. |
2 | Heat phase AB to 85°C and then add phase C ingredients with mixing. |
3 | To the main vessel add the Water of phase D, start mixing, add the Disodium EDTA, then add the Pemulen ® TR-2, and heat this phase to 80°C. |
4 | When both phases ABC and D are homogeneous and at designated temperatures, slowly add phase ABC to phase D with mixing. |
5 | Start homogenizing intensively for 3 minutes and start cooling with continued homogenization. When the batch is at 55°C add phase E. |
6 | Stop homogenizing and resume sweep mixing. Add phase F premix, mix well and then add phase G. |
7 | When the batch is uniform add deionized water to correct for evaporative losses. Continue mixing until smooth. |
Appearance | Off-white lotion |
Viscosity (Brk, RVDV-II, T-D, 20 rpm, after 24 h at room temperature; mPa∙s) | 4000 - 7000 |
pH | 5.5 - 6.5 |
*Patented and Patent Pending
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