This natural (mineral UV filters only) oil-in-water global sunscreen cream formulation was designed to provide broad spectrum (SPF/PFA ≤3) label SPF 50 performance. HallBrite® BHB (Butyloctyl Salicylate) in HallBrite® EZ-FLO TDX, in combination with Biochemica® Bio Vera Aloe Oil, Biochemica® Avocado Butter, and Biochemica® Shea Butter, enhances product feel. It was subjected to in vitro analysis and delivered SPF ~53, PFA (PPD) ~18 performance with critical wavelength 375 nm.
Phase | INCI Name [INN/USAN] (Other Information) | Trade Name | % Wt | Function |
---|---|---|---|---|
A | Persea Gratissima (Avocado) Oil, Hydrogenated Vegetable Oil | BIOCHEMICA® AVOCADO BUTTER | 2.00 | Emollient |
Aloe Barbadensis Leaf Extract, Canola Oil | BIOCHEMICA® BIOVERA ALOE OIL | 6.00 | Emollient | |
Butyrospermum Parkii (Shea) Butter | BIOCHEMICA® SHEA BUTTER REFINED | 0.30 | Emollient | |
Tocopheryl Acetate | 0.30 | Antioxidant Agent | ||
Butyloctyl Salicylate, Titanium Dioxide (nano) [Titanium Dioxide] (40%), Triceteareth-4 Phosphate, Dimethicone Crosspolymer, Silica | HALLBRITE® EZ-FLO TDX | 8.00 | UV Filter/Sunscreen Agent / Carrier System | |
B | Zinc Oxide [Zinc Oxide], Triethoxycaprylylsilane (30-200 nm primary particle size) | 17.00 | UV Filter / Sunscreen Agent | |
C | VP/Eicosene Copolymer | 2.00 | Film Former | |
Glyceryl Stearate | HALLSTAR® GMS PURE | 3.00 | Emulsifier | |
PEG-100 Stearate | HALLSTAR® PEG 4400 MS | 2.80 | Co-emulsifier | |
D | Water (Aqua) | up to 100 | Volatile Carrier | |
Glycerin | 3.00 | Humectant | ||
Disodium EDTA | 0.05 | Chelating Agent | ||
Xanthan Gum (pharma grade) | 0.35 | Thickener (Aqueous) | ||
E | Caprylyl Glycol, Phenoxyethanol, Hexylene Glycol | a.n. | Preservative | |
Cyclopentasiloxane | 2.00 | Emollient | ||
Aluminum Starch Octenylsuccinate | 2.00 | Deoiling Agent |
1 | To a secondary vessel add phase A and start mixing, add phase B and heat to 80°C. |
2 | Add phase C into phase AB, mixing well until all are dissolved, and then homogenize for 3 minutes. |
3 | To the main vessel add the Water and Glycerin of phase D, start mixing and add remaining phase items in order. |
4 | When solids of phase D are fully incorporated, heat phase to 75°C. |
5 | When both phases are homogeneous and at their designated temperatures, slowly add phase ABC to phase D with prop mixing. |
6 | When both phases are homogeneous and at their designated temperatures, slowly add phase ABC to phase D with prop mixing. |
7 | Continue mixing until batch is at room temperature, replacing any water lost to evaporation and mixing until smooth. |
Appearance | Off white cream |
Viscosity (Brk, DVII, T-D, 20 rpm, after 24 h at room temperature; mPa∙s) | 10000 - 15000 |
pH (as is) | 6.5 - 7.5 |
*Patented and Patent Pending
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